Technology Process of Z-MeA2bu(γPht)-OH
There total 5 articles about Z-MeA2bu(γPht)-OH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylsilane;
In
chloroform; trifluoroacetic acid;
for 24h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 67 percent / acetonitrile / 48 h / Ambient temperature
2: 100 percent / TsOH*H2O / toluene / 1 h / Heating
3: 100 percent / Et3SiH / trifluoroacetic acid; CHCl3 / 24 h / Ambient temperature
With
triethylsilane; toluene-4-sulfonic acid;
In
chloroform; toluene; acetonitrile; trifluoroacetic acid;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 103 percent / (CF3COO)2-I-Ph, pyridine / 24 h / Ambient temperature
2: 67 percent / acetonitrile / 48 h / Ambient temperature
3: 100 percent / TsOH*H2O / toluene / 1 h / Heating
4: 100 percent / Et3SiH / trifluoroacetic acid; CHCl3 / 24 h / Ambient temperature
With
pyridine; triethylsilane; toluene-4-sulfonic acid; bis-[(trifluoroacetoxy)iodo]benzene;
In
chloroform; toluene; acetonitrile; trifluoroacetic acid;