Technology Process of Z-MeA2bu(γPht)-O-tBu
There total 6 articles about Z-MeA2bu(γPht)-O-tBu which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 67 percent / acetonitrile / 48 h / Ambient temperature
2: 100 percent / TsOH*H2O / toluene / 1 h / Heating
3: 100 percent / Et3SiH / trifluoroacetic acid; CHCl3 / 24 h / Ambient temperature
4: 81 percent / HBr / acetic acid / 1 h / Ambient temperature
5: H2SO4 / CH2Cl2
With
triethylsilane; sulfuric acid; hydrogen bromide; toluene-4-sulfonic acid;
In
dichloromethane; chloroform; acetic acid; toluene; acetonitrile; trifluoroacetic acid;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 103 percent / (CF3COO)2-I-Ph, pyridine / 24 h / Ambient temperature
2: 67 percent / acetonitrile / 48 h / Ambient temperature
3: 100 percent / TsOH*H2O / toluene / 1 h / Heating
4: 100 percent / Et3SiH / trifluoroacetic acid; CHCl3 / 24 h / Ambient temperature
5: 81 percent / HBr / acetic acid / 1 h / Ambient temperature
6: H2SO4 / CH2Cl2
With
pyridine; triethylsilane; sulfuric acid; hydrogen bromide; toluene-4-sulfonic acid; bis-[(trifluoroacetoxy)iodo]benzene;
In
dichloromethane; chloroform; acetic acid; toluene; acetonitrile; trifluoroacetic acid;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 67 percent / acetonitrile / 48 h / Ambient temperature
2: 100 percent / TsOH*H2O / toluene / 1 h / Heating
3: 100 percent / Et3SiH / trifluoroacetic acid; CHCl3 / 24 h / Ambient temperature
4: 81 percent / HBr / acetic acid / 1 h / Ambient temperature
5: H2SO4 / CH2Cl2
With
triethylsilane; sulfuric acid; hydrogen bromide; toluene-4-sulfonic acid;
In
dichloromethane; chloroform; acetic acid; toluene; acetonitrile; trifluoroacetic acid;