((3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-phenylethynyl-silane

Base Information

Chemical Name:((3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-phenylethynyl-silane
CAS No.:135560-95-1
Molecular Formula:C₄₃H₄₄O₅SeSi
Molecular Weight:747.865
Hs Code.:

Synonyms:((3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-phenylethynyl-silane

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Chemical Property of ((3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-phenylethynyl-silane

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Technology Process of ((3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-phenylethynyl-silane

There total 2 articles about ((3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-phenylethynyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135583-76-5
Acetic acid (3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yl ester

: 135560-95-1
((3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-phenylethynyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: methoxide / methanol

With methanolate; In methanol;
DOI:10.1021/ja00018a063

Reference yield:

: 42591-54-8
chlorodimethyl(phenylethynyl)silane

: 135636-96-3
(3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-ol

: 135560-95-1
((3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-phenylethynyl-silane

Guidance literature:: DOI:10.1021/ja00018a063

Reference yield:

: 135560-95-1
((3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-phenylethynyl-silane

: 135560-96-2,135636-97-4,135636-98-5,135637-05-7
(2R,3S,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-((E)-styryl)-tetrahydro-pyran-3-ol

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; Yield given. Multistep reaction; 1.) benzene, reflux, 2.) THF;
DOI:10.1021/ja00018a063