ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-4-nitrophenylcarbamate

Base Information

Chemical Name:ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-4-nitrophenylcarbamate
CAS No.:1620090-35-8
Molecular Formula:C₂₀H₂₀IN₃O₆S
Molecular Weight:557.366
Hs Code.:

Synonyms:ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-4-nitrophenylcarbamate

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Chemical Property of ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-4-nitrophenylcarbamate

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Technology Process of ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-4-nitrophenylcarbamate

There total 2 articles about ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-4-nitrophenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620090-30-3
ethyl-2-(4-(4-methylphenylsulfonamido)but-1-ynyl)-4-nitrophenylcarbamate

: 1620090-35-8
ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-4-nitrophenylcarbamate

Guidance literature:: With iodine; potassium carbonate; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c4cc02466d

Reference yield:

: 161040-05-7
N-(but-3-yn-1-yl)-4-methylbenzenesulfonamide

: 766518-95-0
ethyl N-(2-iodo-4-nitrophenyl)carbamate

: 1620090-35-8
ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-4-nitrophenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / triethylamine / 6 h / 20 °C

2: potassium carbonate; iodine / acetonitrile / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; iodine; potassium carbonate; In triethylamine; acetonitrile;
DOI:10.1039/c4cc02466d

Reference yield: 61.0%

: 1620090-35-8
ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-4-nitrophenylcarbamate

: ethyl 7-nitro-1-tosyl-2,3-dihydropyrrolo[3,2-b]indole-4(1H)-carboxylate

Guidance literature:: With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; In toluene; at 110 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2016.09.044