Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine

Base Information

Chemical Name:Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine
CAS No.:108607-44-9
Molecular Formula:C₅₅H₆₂N₈O₁₂S₂
Molecular Weight:1091.28
Hs Code.:

Synonyms:Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine

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Chemical Property of Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine

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Technology Process of Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine

There total 12 articles about Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 108607-43-8
Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

: 108607-44-9
Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine

Guidance literature:: With iron(III) chloride; In water; N,N-dimethyl-formamide; at 35 ℃; for 0.5h;

Reference yield:

: 39621-64-2
S-benzyl-N-[(benzyloxy)carbonyl]cysteinyltyrosine

: 108607-44-9
Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / CaCl₂, thermolysin / dimethylformamide; various solvent(s) / 24 h / 38 °C / pH 7.0

2: 74 percent / 1 M NaOH / dioxane / 3 h / Ambient temperature

3: 64 percent / α-chymotrypsin / dimethylformamide; various solvent(s) / 20 h / 38 °C / pH 7

4: 59 percent / ferric chloride / dimethylformamide; H₂O / 0.5 h / 35 °C

With sodium hydroxide; iron(III) chloride; calcium chloride; α-chymotrypsin; thermolysin; In 1,4-dioxane; water; N,N-dimethyl-formamide;

Reference yield:

: phenylalanine phenylhydrazide trifluoroacetate

: 108607-44-9
Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / CaCl₂, thermolysin / dimethylformamide; various solvent(s) / 6 h / 38 °C / pH 7.0

2: 62 percent / ferric chloride / dioxane; H₂O / 0.5 h / 35 °C

3: 64 percent / α-chymotrypsin / dimethylformamide; various solvent(s) / 20 h / 38 °C / pH 7

4: 59 percent / ferric chloride / dimethylformamide; H₂O / 0.5 h / 35 °C

With iron(III) chloride; calcium chloride; α-chymotrypsin; thermolysin; In 1,4-dioxane; water; N,N-dimethyl-formamide;