(2S,5S)-2-Benzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

Base Information

Chemical Name:(2S,5S)-2-Benzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol
CAS No.:155099-13-1
Molecular Formula:C₂₄H₃₁NO₃
Molecular Weight:381.515
Hs Code.:

Synonyms:(2S,5S)-2-Benzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,5S)-2-Benzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

Chemical Property:

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Technology Process of (2S,5S)-2-Benzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

There total 4 articles about (2S,5S)-2-Benzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2612-30-8
2-benzyl-1,3-propanediol

: 155099-13-1
(2S,5S)-2-Benzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / CH₂Cl₂ / Ambient temperature

2: DMSO, oxalyl chloride, diisopropylethylamine / CH₂Cl₂ / -78 deg C, 30 min then warm to room temp.

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo00084a037

Reference yield:

: 49769-78-0
2-benzyl-malonic acid dimethyl ester

: 155099-13-1
(2S,5S)-2-Benzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / LiAlH₄ / diethyl ether / Ambient temperature

2: triethylamine / CH₂Cl₂ / Ambient temperature

3: DMSO, oxalyl chloride, diisopropylethylamine / CH₂Cl₂ / -78 deg C, 30 min then warm to room temp.

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jo00084a037

Reference yield:

: 100-39-0
benzyl bromide

: 155099-13-1
(2S,5S)-2-Benzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / K₂CO₃ / acetone / Heating

2: 100 percent / LiAlH₄ / diethyl ether / Ambient temperature

3: triethylamine / CH₂Cl₂ / Ambient temperature

4: DMSO, oxalyl chloride, diisopropylethylamine / CH₂Cl₂ / -78 deg C, 30 min then warm to room temp.

With lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; acetone;
DOI:10.1021/jo00084a037