3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl

Base Information

Chemical Name:3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl
CAS No.:1395237-89-4
Molecular Formula:C₆₈H₈₈O₁₂Si₃
Molecular Weight:1181.7
Hs Code.:

3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl

Synonyms:3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl

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Chemical Property of 3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl

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Technology Process of 3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl

There total 5 articles about 3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1873-88-7
1,1,1,3,5,5,5-heptamethyltrisiloxan

: 3′-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-(10-undecenyloxy)benzoyloxy]benzoyloxy}biphenyl

: 1395237-89-4
3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl

Guidance literature:: With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In toluene; at 20 ℃; for 48h;
DOI:10.1016/j.molliq.2017.04.114

Reference yield:

: 1873-88-7
1,1,1,3,5,5,5-heptamethyltrisiloxan

: 1395238-03-5
C₆₁H₆₆O₁₀

: 1395237-89-4
3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl

Guidance literature:: With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In toluene; at 20 ℃; for 48h;
DOI:10.1039/c2sm25763g

Reference yield:

: C₂₄H₃₀O₄

: 1395237-89-4
3'-{4-[4-(3,7-dimethyloctyloxy)benzoyloxy]benzoyloxy}-4-{4-[4-[11-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)undec-1-yloxy]benzoyloxy]benzoyloxy}biphenyl

Guidance literature:: Multi-step reaction with 5 steps

1: sodium chlorite

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C

3: palladium on activated charcoal; hydrogen / tetrahydrofuran / 18 h / 40 °C

4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C

5: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / toluene / 48 h / 20 °C

With dmap; sodium chlorite; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; palladium on activated charcoal; hydrogen; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c2sm25763g