5-((2,6-dimethylphenyl)(hydroxy)methyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide

Base Information

Chemical Name:5-((2,6-dimethylphenyl)(hydroxy)methyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide
CAS No.:1608112-43-1
Molecular Formula:C₂₅H₂₉NO₆
Molecular Weight:439.508
Hs Code.:

Synonyms:5-((2,6-dimethylphenyl)(hydroxy)methyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide

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Chemical Property of 5-((2,6-dimethylphenyl)(hydroxy)methyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide

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Technology Process of 5-((2,6-dimethylphenyl)(hydroxy)methyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide

There total 4 articles about 5-((2,6-dimethylphenyl)(hydroxy)methyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1608112-70-4
5-(2,6-dimethylbenzoyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide

: 1608112-43-1
5-((2,6-dimethylphenyl)(hydroxy)methyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201301238 DOI:10.1002/ejoc.201301238

Reference yield:

: C₁₄H₁₁ClO₃

: 1608112-43-1
5-((2,6-dimethylphenyl)(hydroxy)methyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; triethylamine; In methanol;
DOI:10.1002/ejoc.201301238

Reference yield:

: 1608112-69-1
C₁₄H₁₂O₄

: 1608112-43-1
5-((2,6-dimethylphenyl)(hydroxy)methyl)-N-ethyl-N-(3,4,5-trimethoxyphenyl)furan-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 3 h / Reflux; Inert atmosphere

2: triethylamine / Inert atmosphere

3: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; thionyl chloride; triethylamine; In methanol;
DOI:10.1002/ejoc.201301238