O₆-benzyl-8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine

Base Information

• Chemical Name: O₆-benzyl-8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine
• CAS No.: 1068435-06-2
• Molecular Formula: C₃₇H₅₆N₆O₄Si₂
• Molecular Weight: 705.06

Synonyms:O₆-benzyl-8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine

Chemical Property of O₆-benzyl-8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine

Chemical Property:

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Technology Process of O₆-benzyl-8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine

There total 1 articles about O₆-benzyl-8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

3,5-dimethylaminoaniline (108-69-0) + O6-benzyl-8-bromo-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine (479408-22-5) → O6-benzyl-8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine (1068435-06-2)

Guidance literature:

With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,2-dimethoxyethane; at 80 ℃; for 72h; Inert atmosphere;

DOI:10.1002/chem.200800979

Reference yield: 78.0%

O6-benzyl-8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine (1068435-06-2) → 8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine (1124321-48-7)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/chem.200800979

Reference yield:

O6-benzyl-8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine (1068435-06-2) → C30H50N6O4Si2 (1124321-48-7)

Guidance literature:

palladium on activated charcoal; In methanol; at 20 ℃;

DOI:10.1080/15257770701490738

upstream raw materials:

3,5-dimethylaminoaniline

O⁶-benzyl-8-bromo-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine

Downstream raw materials:

C₃₀H₅₀N₆O₄Si₂

8N-(3,5-dimethylphenylamino)-3',5'-bis(tert-butyldimethylsilyl)-2'-deoxyguanosine

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