N--4-oxoisoxazolidine

Base Information

Chemical Name:N--4-oxoisoxazolidine
CAS No.:80042-03-1
Molecular Formula:C₁₂H₁₁NO₅
Molecular Weight:249.223
Hs Code.:

N-<o-(carbomethoxy)benzoyl>-4-oxoisoxazolidine

Synonyms:N--4-oxoisoxazolidine

Suppliers and Price of N--4-oxoisoxazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N--4-oxoisoxazolidine

Chemical Property:

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Technology Process of N--4-oxoisoxazolidine

There total 4 articles about N--4-oxoisoxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 80041-99-2
N--4-hydroxyisoxazolidine

: 80042-03-1
N--4-oxoisoxazolidine

Guidance literature:: With pyridine; chromium(VI) oxide; In dichloromethane; for 0.25h; Ambient temperature;
DOI:10.1055/s-1982-29825

Reference yield:

: 80042-02-0
N-<(3-bromo-2-hydroxypropyl)oxy>phthalimide

: 80042-03-1
N--4-oxoisoxazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / t-Butylamine / 1 h / Ambient temperature

2: 50 percent / CrO₃, pyridine / CH₂Cl₂ / 0.25 h / Ambient temperature

With pyridine; chromium(VI) oxide; tert-butylamine; In dichloromethane;
DOI:10.1055/s-1982-29825

Reference yield:

: 524-38-9
N-hydroxyphthalimide

: 80042-03-1
N--4-oxoisoxazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 35 percent / Et₃N / dimethylformamide / 12 h

2: HBr / CHCl₃ / 1 h

3: 100 percent / tert-BuNH₂ / 1 h / Ambient temperature

4: 45 percent / pyridinium dichromate / CH₂Cl₂ / 15 h / Heating

With dipyridinium dichromate; hydrogen bromide; tert-butylamine; triethylamine; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo00342a029