2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester

Base Information

Chemical Name:2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester
CAS No.:174583-27-8
Molecular Formula:C₃₂H₃₂N₂O₆
Molecular Weight:540.616
Hs Code.:

Synonyms:2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester

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Chemical Property of 2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester

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Technology Process of 2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester

There total 1 articles about 2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 20605-01-0
diethyl bis(hydroxymethyl)malonate

: 135098-44-1
1-benzyl-4,5-diphenylimidazole-2-carboxaldehyde

: 174583-27-8
2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester

Guidance literature:: With pyridinium p-toluenesulfonate; for 36h; Heating;
DOI:10.1021/jm9505876

Reference yield: 73.0%

: 174583-27-8
2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester

: 135098-43-0
1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1021/jm9505876

Reference yield:

: 174583-27-8
2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester

: 2-(4,5-diphenylimidazol-2-yl)-5,5-bis(hydroxymethyl)-1,3-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / Ambient temperature

2: 65 percent / liq. ammonia, sodium metal / tetrahydrofuran / 0.83 h / Heating

With lithium aluminium tetrahydride; ammonia; sodium; In tetrahydrofuran;
DOI:10.1021/jm9505876