[ruthenium(II)(η6-1-i-Pr-4-C6H4Me)Cl2(κ1-P-2-diphenylphosphinobenzaldehyde)]

Base Information

Chemical Name:[ruthenium(II)(η6-1-i-Pr-4-C6H4Me)Cl2(κ1-P-2-diphenylphosphinobenzaldehyde)]
CAS No.:686353-40-2
Molecular Formula:C₂₉H₂₉Cl₂OPRu
Molecular Weight:596.498
Hs Code.:

Synonyms:[ruthenium(II)(η6-1-i-Pr-4-C6H4Me)Cl2(κ1-P-2-diphenylphosphinobenzaldehyde)]

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Chemical Property of [ruthenium(II)(η6-1-i-Pr-4-C6H4Me)Cl2(κ1-P-2-diphenylphosphinobenzaldehyde)]

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Technology Process of [ruthenium(II)(η6-1-i-Pr-4-C6H4Me)Cl2(κ1-P-2-diphenylphosphinobenzaldehyde)]

There total 1 articles about [ruthenium(II)(η6-1-i-Pr-4-C6H4Me)Cl2(κ1-P-2-diphenylphosphinobenzaldehyde)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 50777-76-9
(2-formylphenyl)(diphenyl)phosphine

: 686353-40-2
[ruthenium(II)(η6-1-i-Pr-4-C6H4Me)Cl2(κ1-P-2-diphenylphosphinobenzaldehyde)]

Guidance literature:: In dichloromethane; under N2; slurry of Ru complex and ligand (molar ratio 1:2.4) in CH2Cl2 stirred at room temp. for 2 h; filtered through Kieselguhr; filtrate evapd. to dryness; washed with hexane-Et2O; vac. dried; elem. anal.;
DOI:10.1016/S0020-1693(03)00404-3

Reference yield: 95.0%

: 26042-64-8
silver hexafluoroantimonate

: 686353-40-2
[ruthenium(II)(η6-1-i-Pr-4-C6H4Me)Cl2(κ1-P-2-diphenylphosphinobenzaldehyde)]

: 67-64-1
acetone

: [ruthenium(II)(η6-1-i-Pr-4-C6H4Me)(κ1-O-Me2CO)(κ2-P,O-2-diphenylphosphinobenzaldehyde)][SbF6]2

Guidance literature:: In dichloromethane; acetone; under N2; slurry of Ru complex and AgSbF6 (molar ratio 1:2.2) in CH2Cl2 stirred in the dark at room temp. for 1 h; acetone added; filtered through Kieselguhr; filtrate evapd.; Et2O added; ppt. washed with Et2O; vac. dried; elem. anal.;
DOI:10.1016/S0020-1693(03)00404-3