4-heptylbenzoic acid 4-formylphenyl ester

Base Information

• Chemical Name: 4-heptylbenzoic acid 4-formylphenyl ester
• CAS No.: 503446-72-8
• Molecular Formula: C₂₁H₂₄O₃
• Molecular Weight: 324.42
• Mol file: 503446-72-8.mol

Synonyms:4-heptylbenzoic acid 4-formylphenyl ester

Chemical Property of 4-heptylbenzoic acid 4-formylphenyl ester

Chemical Property:

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Technology Process of 4-heptylbenzoic acid 4-formylphenyl ester

There total 1 articles about 4-heptylbenzoic acid 4-formylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4-heptylbenzoic acid (38350-87-7) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 4-heptylbenzoic acid 4-formylphenyl ester (503446-72-8)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 12h;

DOI:10.1080/15421400802198268

Reference yield: 86.0%

2,3,4-trifluoroaniline (3862-73-5) + 4-heptylbenzoic acid 4-formylphenyl ester (503446-72-8) → 6APE

Guidance literature:

With acetic acid; In ethanol; for 7h; Reflux;

DOI:10.1080/15421400802198268

Reference yield: 4.0%

2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate (14538-51-3,78375-92-5) + 4-heptylbenzoic acid 4-formylphenyl ester (503446-72-8) → C27H35N2O4

Guidance literature:

2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate; 4-heptylbenzoic acid 4-formylphenyl ester; With potassium carbonate; In methanol; at 20 ℃; for 24h;

With sodium periodate; In methanol; for 0.05h; Further stages.;

DOI:10.1021/jo0206972

upstream raw materials:

4-heptylbenzoic acid

4-hydroxy-benzaldehyde