9H-9-Fluorenylmethyl N-{2-[4-(4-aminobutyl)phenyl]ethyl} carbamate TFA salt

Base Information

Chemical Name:9H-9-Fluorenylmethyl N-{2-[4-(4-aminobutyl)phenyl]ethyl} carbamate TFA salt
CAS No.:1453473-52-3
Molecular Formula:C₂HF₃O₂*C₂₇H₃₀N₂O₂
Molecular Weight:528.571
Hs Code.:

Synonyms:9H-9-Fluorenylmethyl N-{2-[4-(4-aminobutyl)phenyl]ethyl} carbamate TFA salt

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Chemical Property of 9H-9-Fluorenylmethyl N-{2-[4-(4-aminobutyl)phenyl]ethyl} carbamate TFA salt

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Technology Process of 9H-9-Fluorenylmethyl N-{2-[4-(4-aminobutyl)phenyl]ethyl} carbamate TFA salt

There total 8 articles about 9H-9-Fluorenylmethyl N-{2-[4-(4-aminobutyl)phenyl]ethyl} carbamate TFA salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1453473-49-8
9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate

: 2712-78-9
bis-[(trifluoroacetoxy)iodo]benzene

: 1453473-52-3
9H-9-Fluorenylmethyl N-{2-[4-(4-aminobutyl)phenyl]ethyl} carbamate TFA salt

Guidance literature:: With pyridine; In water; acetonitrile; at 60 ℃;
DOI:10.1002/cmdc.201200470

Reference yield:

: 26011-68-7
methyl N-(2-phenylethyl)carbamate

: 1453473-52-3
9H-9-Fluorenylmethyl N-{2-[4-(4-aminobutyl)phenyl]ethyl} carbamate TFA salt

Guidance literature:: Multi-step reaction with 8 steps

1.1: aluminum (III) chloride / dichloromethane / 12 h / 20 °C

2.1: water; lithium hydroxide / methanol / 20 °C

3.1: trifluoroacetic acid; Propyl-diethylsilan / 55 - 60 °C

4.1: hydrazine hydrate / Reflux

4.2: 3 h / Reflux

5.1: 1,4-dioxane / 12 h / 20 °C

6.1: pyridine; oxalyl dichloride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

7.1: ammonia / tetrahydrofuran / 1 h / 15 - 20 °C

8.1: pyridine / water; acetonitrile / 60 °C

With pyridine; aluminum (III) chloride; oxalyl dichloride; Propyl-diethylsilan; ammonia; water; hydrazine hydrate; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile; 1.1: |Friedel-Crafts Acylation / 4.1: |Wolff-Kishner Reduction / 4.2: |Wolff-Kishner Reduction;
DOI:10.1002/cmdc.201200470

Reference yield:

: 1453473-41-0
5-(4-{2-[(methoxycarbonyl)amino]ethyl}phenyl)-5-oxopentanoic acid

: 1453473-52-3
9H-9-Fluorenylmethyl N-{2-[4-(4-aminobutyl)phenyl]ethyl} carbamate TFA salt

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid; Propyl-diethylsilan / 55 - 60 °C

2.1: hydrazine hydrate / Reflux

2.2: 3 h / Reflux

3.1: 1,4-dioxane / 12 h / 20 °C

4.1: pyridine; oxalyl dichloride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

5.1: ammonia / tetrahydrofuran / 1 h / 15 - 20 °C

6.1: pyridine / water; acetonitrile / 60 °C

With pyridine; oxalyl dichloride; Propyl-diethylsilan; ammonia; hydrazine hydrate; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; water; acetonitrile; 2.1: |Wolff-Kishner Reduction / 2.2: |Wolff-Kishner Reduction;
DOI:10.1002/cmdc.201200470