9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate

Base Information

Chemical Name:9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate
CAS No.:1453473-49-8
Molecular Formula:C₂₈H₃₀N₂O₃
Molecular Weight:442.558
Hs Code.:

Synonyms:9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate

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Chemical Property of 9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate

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Technology Process of 9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate

There total 8 articles about 9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₂₈ClNO₃

: 1453473-49-8
9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate

Guidance literature:: With ammonia; In tetrahydrofuran; at 15 - 20 ℃; for 1h;
DOI:10.1002/cmdc.201200470

Reference yield:

: 26011-68-7
methyl N-(2-phenylethyl)carbamate

: 1453473-49-8
9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate

Guidance literature:: Multi-step reaction with 7 steps

1.1: aluminum (III) chloride / dichloromethane / 12 h / 20 °C

2.1: water; lithium hydroxide / methanol / 20 °C

3.1: trifluoroacetic acid; Propyl-diethylsilan / 55 - 60 °C

4.1: hydrazine hydrate / Reflux

4.2: 3 h / Reflux

5.1: 1,4-dioxane / 12 h / 20 °C

6.1: pyridine; oxalyl dichloride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

7.1: ammonia / tetrahydrofuran / 1 h / 15 - 20 °C

With pyridine; aluminum (III) chloride; oxalyl dichloride; Propyl-diethylsilan; ammonia; water; hydrazine hydrate; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; 1.1: |Friedel-Crafts Acylation / 4.1: |Wolff-Kishner Reduction / 4.2: |Wolff-Kishner Reduction;
DOI:10.1002/cmdc.201200470

Reference yield:

: 1453473-41-0
5-(4-{2-[(methoxycarbonyl)amino]ethyl}phenyl)-5-oxopentanoic acid

: 1453473-49-8
9H-9-fluorenylmethyl N-{2-[4-(5-amino-5-oxopentyl)phenyl]ethyl}carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid; Propyl-diethylsilan / 55 - 60 °C

2.1: hydrazine hydrate / Reflux

2.2: 3 h / Reflux

3.1: 1,4-dioxane / 12 h / 20 °C

4.1: pyridine; oxalyl dichloride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

5.1: ammonia / tetrahydrofuran / 1 h / 15 - 20 °C

With pyridine; oxalyl dichloride; Propyl-diethylsilan; ammonia; hydrazine hydrate; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; 2.1: |Wolff-Kishner Reduction / 2.2: |Wolff-Kishner Reduction;
DOI:10.1002/cmdc.201200470