(methyl)2NHBH₂PH(phenyl)BH₃

Base Information

Chemical Name:(methyl)2NHBH₂PH(phenyl)BH₃
CAS No.:666857-16-5
Molecular Formula:C₈H₁₈B₂NP
Molecular Weight:180.833
Hs Code.:

(methyl)2NHBH<sub>2</sub>PH(phenyl)BH<sub>3</sub>

Synonyms:(methyl)2NHBH₂PH(phenyl)BH₃

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Chemical Property of (methyl)2NHBH₂PH(phenyl)BH₃

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Technology Process of (methyl)2NHBH₂PH(phenyl)BH₃

There total 1 articles about (methyl)2NHBH₂PH(phenyl)BH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 856617-73-7
phenylphosphine borane complex

: Me₂NH*BH₂Cl

: 666857-16-5
(methyl)2NHBH₂PH(phenyl)BH₃

Guidance literature:: With n-butyllithium; In tetrahydrofuran; byproducts: LiCl; N2; dropwise addn. of n-butyllithium in hexanes to THF soln. of (C6H5)2PH*BH3 at 0°C, stirring at this temp. for 30 min, warming to 25°C, cooling to 0°C after 2 h, dropwise addn. of (CH3)2NH*BH2Cl, stirring overnight at 25°C; solvent removal in vac., dissolving in toluene, filtration, solvent removal, washing the solid with hexanes, extn. with ether, recrystn. from toluene/hexanes at -30°C; elem. anal.;
DOI:10.1021/ic034938f

Reference yield: 99.0%

: 666857-16-5
(methyl)2NHBH₂PH(phenyl)BH₃

: 666857-23-4
phenylphosphine borane

Guidance literature:: In neat (no solvent); byproducts: [(CH3)2NBH2]2; N2; heating neat sample of amine-phosphine-borate at 130°C for 2 h; evacuation at 25°C for 24 h;
DOI:10.1021/ic034938f

Reference yield:

: 666857-16-5
(methyl)2NHBH₂PH(phenyl)BH₃

: 856617-73-7
phenylphosphine borane complex

: dimethylamine borane

Guidance literature:: chloro(1,5-cyclooctadiene)rhodium(I) dimer; In toluene; N2; addn. of Ru complex (1.5 mol. %) to toluene soln. of amine-phosphine-borane adduct, heating to 50°C for 10 d; not isolated, detected by NMR;
DOI:10.1021/ic034938f