4-benzoyl-9,10-dioxo-9,10-dihydro-anthracene-1-carboxylic acid

Base Information

• Chemical Name: 4-benzoyl-9,10-dioxo-9,10-dihydro-anthracene-1-carboxylic acid
• CAS No.: 866997-52-6
• Molecular Formula: C₂₂H₁₂O₅
• Molecular Weight: 356.334
• Mol file: 866997-52-6.mol

Synonyms:4-benzoyl-9,10-dioxo-9,10-dihydro-anthracene-1-carboxylic acid

Chemical Property of 4-benzoyl-9,10-dioxo-9,10-dihydro-anthracene-1-carboxylic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-benzoyl-9,10-dioxo-9,10-dihydro-anthracene-1-carboxylic acid

There total 12 articles about 4-benzoyl-9,10-dioxo-9,10-dihydro-anthracene-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

anthracen-9(10H)-one (90-44-8) → 4-benzoyl-9,10-dioxo-9,10-dihydro-anthracene-1-carboxylic acid (866997-52-6)

Guidance literature:

Multi-step reaction with 3 steps

1: aqueous sulfuric acid

2: diethyl ether / anschliessendes Erhitzen in Benzol

3: chromium (VI)-oxide; aqueous acetic acid

With chromium(VI) oxide; diethyl ether; sulfuric acid; acetic acid;

DOI:10.1080/00049530108255130

Reference yield:

6-benzyl-benz[de]anthracen-7-one (5082-84-8) → 4-benzoyl-9,10-dioxo-9,10-dihydro-anthracene-1-carboxylic acid (866997-52-6)

Guidance literature:

With chromium(VI) oxide; acetic acid;

DOI:10.1021/ja01307a046

Reference yield:

1-ethyl-4-benzoyl-anthraquinone (502187-64-6) → 4-benzoyl-9,10-dioxo-9,10-dihydro-anthracene-1-carboxylic acid (866997-52-6)

Guidance literature:

With chromium(VI) oxide; acetic acid;

DOI:10.1080/00049530108255130

upstream raw materials:

6-benzyl-benz[de]anthracen-7-one

1-ethyl-4-benzoyl-anthraquinone

acetic acid

1-benzoyl-4-butyl-anthraquinone

Downstream raw materials:

1-benzoylanthraquinone