6-isopropoxy-7-methoxy-1-(3,4,5-trimethoxybenzyl)-3,4-dihydroisoquinoline hydrochloride

Base Information

• Chemical Name: 6-isopropoxy-7-methoxy-1-(3,4,5-trimethoxybenzyl)-3,4-dihydroisoquinoline hydrochloride
• CAS No.: 1213240-92-6
• Molecular Formula: C₂₃H₂₉NO₅*ClH
• Molecular Weight: 435.948

Synonyms:6-isopropoxy-7-methoxy-1-(3,4,5-trimethoxybenzyl)-3,4-dihydroisoquinoline hydrochloride

Chemical Property of 6-isopropoxy-7-methoxy-1-(3,4,5-trimethoxybenzyl)-3,4-dihydroisoquinoline hydrochloride

Chemical Property:

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Technology Process of 6-isopropoxy-7-methoxy-1-(3,4,5-trimethoxybenzyl)-3,4-dihydroisoquinoline hydrochloride

There total 1 articles about 6-isopropoxy-7-methoxy-1-(3,4,5-trimethoxybenzyl)-3,4-dihydroisoquinoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-(3-isopropoxy-4-methoxyphenethyl)-2-(3,4,5-trimethoxyphenyl) acetamide (1213240-90-4) → 6-isopropoxy-7-methoxy-1-(3,4,5-trimethoxybenzyl)-3,4-dihydroisoquinoline hydrochloride (1213240-92-6)

Guidance literature:

With trichlorophosphate; In toluene; at 20 - 80 ℃;

DOI:10.1016/j.ejmech.2009.09.017

Reference yield: 64.0%

6-isopropoxy-7-methoxy-1-(3,4,5-trimethoxybenzyl)-3,4-dihydroisoquinoline hydrochloride (1213240-92-6) + 4-chlorobenzoylmethyl bromide (536-38-9) → 2-(4-chlorophenyl)-8-isopropoxy-9-methoxy-1-(3,4,5-trimethoxyphenyl)-5,6-dihydropyrrolo[2,1-a]isoquinoline (1213240-71-1)

Guidance literature:

With sodium hydrogencarbonate; In acetonitrile; for 8h; Reflux;

DOI:10.1016/j.ejmech.2009.09.017

Reference yield: 58.0%

2-bromo-1-(4'-hydroxyphenyl)-1-ethanone (2491-38-5) + 6-isopropoxy-7-methoxy-1-(3,4,5-trimethoxybenzyl)-3,4-dihydroisoquinoline hydrochloride (1213240-92-6) → 4-(8-isopropoxy-9-methoxy-1-(3,4,5-trimethoxyphenyl)-5,6-dihydropyrrolo[2,1-a]isoquinolin-2-yl)phenol (1213240-75-5)

Guidance literature:

With sodium hydrogencarbonate; In acetonitrile; for 8h; Reflux;

DOI:10.1016/j.ejmech.2009.09.017

upstream raw materials:

N-(3-isopropoxy-4-methoxyphenethyl)-2-(3,4,5-trimethoxyphenyl) acetamide

Downstream raw materials:

8-isopropoxy-2-(3-isopropoxy-4-methoxyphenyl)-9-methoxy-1-(3,4,5-trimethoxyphenyl)-5,6-dihydropyrrolo[2,1-a]isoquinoline

4-(8-isopropoxy-9-methoxy-1-(3,4,5-trimethoxyphenyl)-5,6-dihydropyrrolo[2,1-a]isoquinolin-2-yl)phenol

5-(8-isopropoxy-9-methoxy-1-(3,4,5-trimethoxyphenyl)-5,6-dihydropyrrolo[2,1-a]isoquinolin-2-yl)-2-methoxyphenol

4-(8-isopropoxy-9-methoxy-1-(3,4,5-trimethoxyphenyl)-5,6-dihydropyrrolo[2,1-a]isoquinolin-2-yl)benzene-1,2-diol

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