13-(4-fluorophenyl)-3,3-dimethyl-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Base Information

Chemical Name:13-(4-fluorophenyl)-3,3-dimethyl-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione
CAS No.:1017238-96-8
Molecular Formula:C₂₃H₁₉FN₂O₃
Molecular Weight:390.414
Hs Code.:

Synonyms:13-(4-fluorophenyl)-3,3-dimethyl-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

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Chemical Property of 13-(4-fluorophenyl)-3,3-dimethyl-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

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Technology Process of 13-(4-fluorophenyl)-3,3-dimethyl-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

There total 9 articles about 13-(4-fluorophenyl)-3,3-dimethyl-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1445-69-8
2,3-dihydrophthalazine-1,4-dione

: 459-57-4
4-fluorobenzaldehyde

: 126-81-8
dimedone

: 1017238-96-8
13-(4-fluorophenyl)-3,3-dimethyl-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Guidance literature:: With [4-(1,10-phenanthrolin-1-ium-1-yl)butane-1-sulfonate]₃PW₁₂O₄₀; In water; for 0.0833333h; Reflux; Green chemistry;
DOI:10.1007/s11164-019-03875-4

Reference yield: 95.0%

: 85-44-9
phthalic anhydride

: 459-57-4
4-fluorobenzaldehyde

: 126-81-8
dimedone

: 1017238-96-8
13-(4-fluorophenyl)-3,3-dimethyl-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Guidance literature:: With hydrazine hydrate; In neat (no solvent); at 80 ℃; for 0.333333h;
DOI:10.1039/c6ra06376d

Reference yield: 93.0%

: 1445-69-8
2,3-dihydrophthalazine-1,4-dione

: 3471-13-4
dimedone

: 459-57-4
4-fluorobenzaldehyde

: 1017238-96-8
13-(4-fluorophenyl)-3,3-dimethyl-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Guidance literature:: With SBA-15 sulfonic acid mesoporous silicas; In acetonitrile; at 45 ℃; for 0.25h; Irradiation; Green chemistry;
DOI:10.1016/j.molcata.2013.03.017