N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylsulphinyl)acetamide

Base Information

• Chemical Name: N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylsulphinyl)acetamide
• CAS No.: 137469-82-0
• Molecular Formula: C₂₅H₂₆N₂O₄S
• Molecular Weight: 450.558

Synonyms:N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylsulphinyl)acetamide

Chemical Property of N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylsulphinyl)acetamide

Chemical Property:

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Technology Process of N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylsulphinyl)acetamide

There total 6 articles about N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylsulphinyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylthio)acetamide (137469-80-8) → N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylsulphinyl)acetamide (137469-82-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 0.666667h; Ambient temperature;

Reference yield:

(phenylthio)acetic acid chloride (7031-27-8) → N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylsulphinyl)acetamide (137469-82-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 93 percent / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

2: 59 percent / Na₂CO₃, Cu / nitrobenzene / 4 h / Heating

3: 87 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.67 h / Ambient temperature

With copper; sodium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; nitrobenzene;

Reference yield:

(phenylthio)acetic acid (103-04-8) → N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylsulphinyl)acetamide (137469-82-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 91 percent / thionyl chloride / 36 h / 20 °C

2: 93 percent / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

3: 59 percent / Na₂CO₃, Cu / nitrobenzene / 4 h / Heating

4: 87 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.67 h / Ambient temperature

With thionyl chloride; copper; sodium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; nitrobenzene;

upstream raw materials:

N-<3-(2-acetylanilino)-6-methoxybenzyl>-N-methyl(phenylthio)acetamide

(phenylthio)acetic acid chloride

(phenylthio)acetic acid

5-bromo-2-methoxy-N-methylbenzylamine

Downstream raw materials:

5-methoxy-3,7-dimethyl-1-phenylthio-3,4-dihydrobenzo-<1,8>phenanthrolin-2(1H)-one

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