3-((4-(methoxycarbonyl)phenoxy)methyl)-4-phenyl-1,2,5-oxadiazole-2-oxide

Base Information

Chemical Name:3-((4-(methoxycarbonyl)phenoxy)methyl)-4-phenyl-1,2,5-oxadiazole-2-oxide
CAS No.:1349820-86-5
Molecular Formula:C₁₇H₁₄N₂O₅
Molecular Weight:326.309
Hs Code.:

Synonyms:3-((4-(methoxycarbonyl)phenoxy)methyl)-4-phenyl-1,2,5-oxadiazole-2-oxide

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Chemical Property of 3-((4-(methoxycarbonyl)phenoxy)methyl)-4-phenyl-1,2,5-oxadiazole-2-oxide

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Technology Process of 3-((4-(methoxycarbonyl)phenoxy)methyl)-4-phenyl-1,2,5-oxadiazole-2-oxide

There total 3 articles about 3-((4-(methoxycarbonyl)phenoxy)methyl)-4-phenyl-1,2,5-oxadiazole-2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.5%

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 217966-10-4
3-chloromethyl-4-phenyl-1,2,5-oxadiazole N²-oxide

: 1349820-86-5
3-((4-(methoxycarbonyl)phenoxy)methyl)-4-phenyl-1,2,5-oxadiazole-2-oxide

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 10h;

Reference yield:

: 104-54-1
3-Phenylpropenol

: 1349820-86-5
3-((4-(methoxycarbonyl)phenoxy)methyl)-4-phenyl-1,2,5-oxadiazole-2-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; sodium nitrite

2: pyridine; thionyl chloride / dichloromethane

3: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C

With pyridine; thionyl chloride; potassium carbonate; acetic acid; potassium iodide; sodium nitrite; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.103

Reference yield:

: 135733-30-1
3-(hydroxymethyl)-4-phenylfuroxan

: 1349820-86-5
3-((4-(methoxycarbonyl)phenoxy)methyl)-4-phenyl-1,2,5-oxadiazole-2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; thionyl chloride / dichloromethane

2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C

With pyridine; thionyl chloride; potassium carbonate; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.103