Technology Process of C34H43BrN6O10
There total 5 articles about C34H43BrN6O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 8h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / dichloromethane / 14 h / 20 °C
2: potassium carbonate / acetonitrile / Inert atmosphere; Reflux
3: sodium hydroxide; water / tetrahydrofuran / 20 h / 45 °C
4: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 8 h / 20 °C / Inert atmosphere
With
pyridine; water; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetonitrile / Inert atmosphere; Reflux
2: sodium hydroxide; water / tetrahydrofuran / 20 h / 45 °C
3: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 8 h / 20 °C / Inert atmosphere
With
water; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; acetonitrile;