3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate

Base Information

Chemical Name:3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate
CAS No.:1265359-33-8
Molecular Formula:C₁₃H₁₂F₄O₆S
Molecular Weight:372.294
Hs Code.:

Synonyms:3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate

Suppliers and Price of 3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate

There total 5 articles about 3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.5%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1265359-31-6
2-fluoro-6-hydroxy-4-(tetrahydro-2H-pyran-2-yloxy) benzaldehyde

: 1265359-33-8
3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate

Guidance literature:: With pyridine; In dichloromethane; at -15 - 20 ℃; for 3h;

Reference yield:

: 52189-63-6
3,5-dimethoxyfluorobenzene

: 1265359-33-8
3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 0 - 20 °C

2: boron tribromide / dichloromethane / -78 - 20 °C

3: pyridinium p-toluenesulfonate / dichloromethane / 20 °C

4: pyridine / dichloromethane / 3 h / -15 - 20 °C

With pyridine; boron tribromide; trichlorophosphate; pyridinium p-toluenesulfonate; In dichloromethane;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1265359-33-8
3-fluoro-2-formyl-5-(tetrahydro-2H-pyran-2-yloxy)phenyltrifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: tetrafluoroboric acid; sodium nitrite / water / 0.5 h / 20 °C

2: trichlorophosphate / 0 - 20 °C

3: boron tribromide / dichloromethane / -78 - 20 °C

4: pyridinium p-toluenesulfonate / dichloromethane / 20 °C

5: pyridine / dichloromethane / 3 h / -15 - 20 °C

With pyridine; tetrafluoroboric acid; boron tribromide; sodium nitrite; trichlorophosphate; pyridinium p-toluenesulfonate; In dichloromethane; water;