2,3-dihydroxypropyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate

Base Information

• Chemical Name: 2,3-dihydroxypropyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate
• CAS No.: 1350724-98-9
• Molecular Formula: C₂₉H₅₀O₆
• Molecular Weight: 494.712
• Mol file: 1350724-98-9.mol

Synonyms:2,3-dihydroxypropyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate

Chemical Property of 2,3-dihydroxypropyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dihydroxypropyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate

There total 4 articles about 2,3-dihydroxypropyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(+/-)-(2,2-dimethyl-1,3-dioxolan-4-yl)methyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate (1350724-64-9) → 2,3-dihydroxypropyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate (1350724-98-9)

Guidance literature:

With acetic acid; In ethanol; water; at 40 - 50 ℃; for 3h;

DOI:10.1021/jm200529h

Reference yield:

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene (60526-81-0) → 2,3-dihydroxypropyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate (1350724-98-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: boron tribromide / dichloromethane

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

3.1: acetic acid / ethanol; water / 3 h / 40 - 50 °C

With potassium fluoride; boron tribromide; potassium carbonate; acetic acid; In ethanol; dichloromethane; water; acetone;

DOI:10.1021/jm200529h

Reference yield:

11-bromoundecanoic acid (2834-05-1) → 2,3-dihydroxypropyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate (1350724-98-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

3.1: acetic acid / ethanol; water / 3 h / 40 - 50 °C

With dmap; potassium fluoride; potassium carbonate; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; water; acetone;

DOI:10.1021/jm200529h

upstream raw materials:

(+/-)-(2,2-dimethyl-1,3-dioxolan-4-yl)methyl 11-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]undecanoate

11-bromoundecanoic acid

5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene