N,N'-dicyclohexyl-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide

Base Information

• Chemical Name: N,N'-dicyclohexyl-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide
• CAS No.: 1193778-04-9
• Molecular Formula: C₂₈H₃₀N₄O₄
• Molecular Weight: 486.571
• Mol file: 1193778-04-9.mol

Synonyms:N,N'-dicyclohexyl-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide

Chemical Property of N,N'-dicyclohexyl-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-dicyclohexyl-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide

There total 2 articles about N,N'-dicyclohexyl-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

N,N'-dicyclohexyl-2,6-dibromonaphthalene-1,4,5,8-tetracarboxylic acid bisimide (1193777-99-9) + ethylenediamine (107-15-3,85404-18-8) → N,N'-dicyclohexyl-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide (1193778-04-9) + N,N'-dicyclohexyl-6-bromo-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide (1193778-03-8)

Guidance literature:

at 25 ℃; for 16h; Neat (no solvent); Inert atmosphere;

DOI:10.1021/jo9017342

Reference yield:

N,N'-dicyclohexyl-6-bromo-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide (1193778-03-8) → N,N'-dicyclohexyl-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide (1193778-04-9)

Guidance literature:

With sodium dithionite; In water; dimethyl sulfoxide; at 40 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jo9017342

Reference yield: 64.0%

N,N'-dicyclohexyl-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide (1193778-04-9) → 2,7-dicyclohexyl-9H,12H-2,7,9,12-tetraaza-benzo[e]pyrene-1,3,6,8,10,11-hexaone (1193778-06-1)

Guidance literature:

With potassium dichromate; sulfuric acid; In water; acetone; at 100 ℃; for 2h;

DOI:10.1021/jo9017342

upstream raw materials:

N,N'-dicyclohexyl-2,6-dibromonaphthalene-1,4,5,8-tetracarboxylic acid bisimide

ethylenediamine

N,N'-dicyclohexyl-6-bromo-5,8,9,10-(1,4-diaza-1,2,3,4-tetrahydroanthracene)tetracarboxylic acid bisimide

Downstream raw materials:

2,7-dicyclohexyl-9H,12H-2,7,9,12-tetraaza-benzo[e]pyrene-1,3,6,8,10,11-hexaone