N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine

Base Information

Chemical Name:N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine
CAS No.:945840-42-6
Molecular Formula:C₂₀H₁₈N₄O₄
Molecular Weight:378.387
Hs Code.:

Synonyms:N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine

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Chemical Property of N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine

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Technology Process of N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine

There total 1 articles about N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 107-15-3,85404-18-8
ethylenediamine

: 1466-88-2,66894-06-2
2-nitrocinnamaldehyde

: 945840-42-6
N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine

Guidance literature:: In methanol; for 3h; Cooling with ice;
DOI:10.1080/15257770.2017.1332763

Reference yield: 95.0%

: 945840-42-6
N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine

: bis(acetonitrile)bis(triphenylphosphine)copper(I) tetraphenylborate

: [Cu(N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine)(triphenylphosphine)2]BPh₄

Guidance literature:: In acetonitrile; 1 equiv. of Cu-compd. was added to MeCN soln. of N-compd., stirring for 20 min at room temp.; soln. was concd. in vac. until appearing of crystals, Et2O was diffundedinto the soln., elem. anal.;
DOI:10.1002/zaac.200600161

Reference yield: 90.0%

: 14057-91-1
tetrakis(acetonitrile)copper(I) perchlorate

: 945840-42-6
N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine

: [Cu(N,N'-bis[3-(2-nitrophenyl)-allylidene]ethane-1,2-diamine)]ClO₄

Guidance literature:: In acetonitrile; 0.5 equiv. of Cu-compd. was added to MeCN soln. of N-compd., stirring for 20 min; soln. was concd. in vac., Et2O was diffunded into the soln., crystals were filtered off, washed with Et2O/MeCN (9:1, v/v), dried in vac., elem. anal.;
DOI:10.1002/zaac.200600161