phenyl 2-[(benzoylamino)carbonyl]oxy-2-phenylethyl selenide

Base Information

• Chemical Name: phenyl 2-[(benzoylamino)carbonyl]oxy-2-phenylethyl selenide
• CAS No.: 951789-33-6
• Molecular Formula: C₂₂H₁₉NO₃Se
• Molecular Weight: 424.358
• Mol file: 951789-33-6.mol

Synonyms:phenyl 2-[(benzoylamino)carbonyl]oxy-2-phenylethyl selenide

Chemical Property of phenyl 2-[(benzoylamino)carbonyl]oxy-2-phenylethyl selenide

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of phenyl 2-[(benzoylamino)carbonyl]oxy-2-phenylethyl selenide

There total 1 articles about phenyl 2-[(benzoylamino)carbonyl]oxy-2-phenylethyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-phenyl-2-(phenylselanyl)ethanol (51558-95-3) + benzoyl isocyanate (4461-33-0) → phenyl 2-[(benzoylamino)carbonyl]oxy-2-phenylethyl selenide (951789-33-6)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1080/00397910701465420

Reference yield:

phenyl 2-[(benzoylamino)carbonyl]oxy-2-phenylethyl selenide (951789-33-6) → C22H19NO5Se

Guidance literature:

With dipotassium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; at 20 ℃;

DOI:10.1080/00397910701465420

Reference yield:

phenyl 2-[(benzoylamino)carbonyl]oxy-2-phenylethyl selenide (951789-33-6) → 5-phenyloxazolidin-2-one (7693-77-8,54705-41-8,60426-44-0)

Guidance literature:

Multi-step reaction with 2 steps

1: m-chloroperbenzoic acid; potassium hydrogen phosphate / tetrahydrofuran / 20 °C

2: aq. HCl / tetrahydrofuran / 4 h / 65 °C

With hydrogenchloride; dipotassium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran;

DOI:10.1080/00397910701465420

upstream raw materials:

1-phenyl-2-(phenylselanyl)ethanol

benzoyl isocyanate

Downstream raw materials:

5-phenyloxazolidin-2-one