6-deoxy-6-iodo-2,3-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

Base Information

Chemical Name:6-deoxy-6-iodo-2,3-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose
CAS No.:83032-12-6
Molecular Formula:C₁₆H₂₁IO₇S
Molecular Weight:484.309
Hs Code.:

Synonyms:6-deoxy-6-iodo-2,3-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-deoxy-6-iodo-2,3-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

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Technology Process of 6-deoxy-6-iodo-2,3-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

There total 7 articles about 6-deoxy-6-iodo-2,3-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 32087-60-8
2,3-O-isopropylidene-1,6-bis-O-(p-tolylsulphonyl)-β-D-fructofuranose

: 83032-12-6
6-deoxy-6-iodo-2,3-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

Guidance literature:: With sodium iodide; In N,N-dimethyl-formamide; at 90 ℃;

Reference yield:

: 2484-55-1
2,3-O-isopropylidene-1,6-bis-O-(p-toluenesulfonyl)-α-L-sorbofuranose

: 83032-12-6
O²,O³-isopropylidene-6-iodo-O¹-(toluene-4-sulfonyl)-6-deoxy-α-L-sorbofuranose

Guidance literature:: With acetone; sodium iodide;
DOI:10.1002/hlca.19380210138

Reference yield:

: 57-48-7,18875-34-8
D-Fructose

: 83032-12-6
6-deoxy-6-iodo-2,3-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; chloroform / Behandeln des Reaktionsprodukts mit Aceton, Kupfer(II)-sulfat und wenig Schwefelsaeure

2: acetone; sodium iodide

With pyridine; chloroform; acetone; sodium iodide;
DOI:10.1002/hlca.193802101132