5-[[(tert-butyldiphenyl)silanyloxy]phenyl]-3-isoxazolecarboxylic acid ethyl ester

Base Information

Chemical Name:5-[[(tert-butyldiphenyl)silanyloxy]phenyl]-3-isoxazolecarboxylic acid ethyl ester
CAS No.:1203611-10-2
Molecular Formula:C₂₈H₂₉NO₄Si
Molecular Weight:471.628
Hs Code.:

Synonyms:5-[[(tert-butyldiphenyl)silanyloxy]phenyl]-3-isoxazolecarboxylic acid ethyl ester

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Chemical Property of 5-[[(tert-butyldiphenyl)silanyloxy]phenyl]-3-isoxazolecarboxylic acid ethyl ester

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Technology Process of 5-[[(tert-butyldiphenyl)silanyloxy]phenyl]-3-isoxazolecarboxylic acid ethyl ester

There total 2 articles about 5-[[(tert-butyldiphenyl)silanyloxy]phenyl]-3-isoxazolecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1203611-09-9
3-[(tert-butyldiphenyl)silanyloxy]phenylacetylene

: 623-33-6
glycine ethyl ester hydrochloride

: 1203611-10-2
5-[[(tert-butyldiphenyl)silanyloxy]phenyl]-3-isoxazolecarboxylic acid ethyl ester

Guidance literature:: With tert.-butylnitrite; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium hydrogencarbonate; zinc dibromide; In tert-butyl methyl ether; at 20 ℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.0c02281