O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine

Base Information

Chemical Name:O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine
CAS No.:79628-29-8
Molecular Formula:C₃₂H₃₆F₁₅N₅O₁₄
Molecular Weight:999.639
Hs Code.:

O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine

Synonyms:O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine

Suppliers and Price of O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine

There total 8 articles about O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.1%

: 70333-69-6
4,5-di-O-acetyl-1,2,3-trideoxy-3-<(trifluoroacetyl)amino>-D-arabino-hex-1-enopyranose

: 70333-74-3
3',4'-dideoxy-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

: 79628-29-8
O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine

Guidance literature:: With boron trifluoride diethyl etherate; In ethyl acetate; for 5h;
DOI:10.1021/jm00144a023

Reference yield:

: 3947-65-7
neomycin A

: 79628-29-8
O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine

Guidance literature:: Multi-step reaction with 7 steps

1: 75.3 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

2: 76.3 percent / CF₃COOH / acetonitrile / 0.75 h / Heating

3: 94.4 percent / pyridine / Ambient temperature

4: NaI, Zn / dimethylformamide / 1.5 h / 95 °C

5: H₂ / PtO₂ / methanol / 18 h

6: 41.3 percent / CH₃COOH, H₂O / 0.25 h / Ambient temperature

7: 26.1 percent / BF₃*Et₂O / ethyl acetate / 5 h

With pyridine; boron trifluoride diethyl etherate; water; hydrogen; acetic acid; triethylamine; trifluoroacetic acid; sodium iodide; zinc; platinum(IV) oxide; In methanol; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00144a023

Reference yield:

: 61066-03-3
1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

: 79628-29-8
O-4,6-diacetyl-2,3-dideoxy-3-<(trifluoroacetyl)amino>-α-D-glucopyranosyl-(1->6)-O-<2,6-bis<(trifluoroacetyl)amino>-2,3,4,6-tetradeoxy-α-D-glucopyranosyl-(1->4)>-2-deoxy-1,3-bis-N-(trifluoroacetyl)-D-streptamine

Guidance literature:: Multi-step reaction with 6 steps

1: 76.3 percent / CF₃COOH / acetonitrile / 0.75 h / Heating

2: 94.4 percent / pyridine / Ambient temperature

3: NaI, Zn / dimethylformamide / 1.5 h / 95 °C

4: H₂ / PtO₂ / methanol / 18 h

5: 41.3 percent / CH₃COOH, H₂O / 0.25 h / Ambient temperature

6: 26.1 percent / BF₃*Et₂O / ethyl acetate / 5 h

With pyridine; boron trifluoride diethyl etherate; water; hydrogen; acetic acid; trifluoroacetic acid; sodium iodide; zinc; platinum(IV) oxide; In methanol; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00144a023