Benzyl 4-[3-acetyl-2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate

Base Information

Chemical Name:Benzyl 4-[3-acetyl-2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate
CAS No.:762173-01-3
Molecular Formula:C₂₈H₂₆FN₃O₃
Molecular Weight:471.531
Hs Code.:

Synonyms:Benzyl 4-[3-acetyl-2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate

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Chemical Property of Benzyl 4-[3-acetyl-2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate

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Technology Process of Benzyl 4-[3-acetyl-2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate

There total 4 articles about Benzyl 4-[3-acetyl-2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 762173-00-2
benzyl 4-[2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate

: 108-24-7
acetic anhydride

: 762173-01-3
Benzyl 4-[3-acetyl-2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate

Guidance literature:: With sulfuric acid; at 125 - 170 ℃; for 84h;

Reference yield:

: 2-chloro-1-(4-fluoro-phenyl)-ethanone O-methyl-oxime

: 762173-01-3
Benzyl 4-[3-acetyl-2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: LiBr

2: potassium tert-butoxide

3: sulfuric acid

With sulfuric acid; potassium tert-butylate; lithium bromide;
DOI:10.1016/j.bmcl.2006.01.092

Reference yield:

: 2-bromo-1-(4-fluorophenyl)ethanone O-methyloxime

: 762173-01-3
Benzyl 4-[3-acetyl-2-(4-fluorophenyl)imidazo[1,2-a]pyridin-7-yl]piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butoxide

2: sulfuric acid

With sulfuric acid; potassium tert-butylate;
DOI:10.1016/j.bmcl.2006.01.092