toluene-4-sulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester
CAS No.:1207529-70-1
Molecular Formula:C₂₂H₂₃ClF₃NO₄S
Molecular Weight:489.943
Hs Code.:

Synonyms:toluene-4-sulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

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Chemical Property of toluene-4-sulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

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Technology Process of toluene-4-sulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

There total 4 articles about toluene-4-sulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207530-03-7
trans-2-chloro-N-(4-hydroxymethyl-cyclohexyl)-5-trifluoromethyl-benzamide

: 98-59-9
p-toluenesulfonyl chloride

: 1207529-70-1
toluene-4-sulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;

Reference yield:

: 657-05-6
2-chloro-5-trifluoromethylbenzoyl chloride

: 1207529-70-1
toluene-4-sulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 1.83 h / 0 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere

2.2: 0 °C

3.1: pyridine / dichloromethane / 20 °C

With pyridine; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 61367-07-5,61367-16-6,100707-54-8
trans-4-aminocyclohexylcarboxylic acid methyl ester hydrochloride

: 1207529-70-1
toluene-4-sulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 1.83 h / 0 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere

2.2: 0 °C

3.1: pyridine / dichloromethane / 20 °C

With pyridine; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;