1-(2,2-dimethyl-6-prop-2-ynyloxytetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-trityloxyethanol

Base Information

Chemical Name:1-(2,2-dimethyl-6-prop-2-ynyloxytetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-trityloxyethanol
CAS No.:1402436-27-4
Molecular Formula:C₃₁H₃₂O₆
Molecular Weight:500.591
Hs Code.:

Synonyms:1-(2,2-dimethyl-6-prop-2-ynyloxytetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-trityloxyethanol

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Chemical Property of 1-(2,2-dimethyl-6-prop-2-ynyloxytetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-trityloxyethanol

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Technology Process of 1-(2,2-dimethyl-6-prop-2-ynyloxytetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-trityloxyethanol

There total 3 articles about 1-(2,2-dimethyl-6-prop-2-ynyloxytetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-trityloxyethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 1402436-27-4
1-(2,2-dimethyl-6-prop-2-ynyloxytetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-trityloxyethanol

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0 - 20 °C

2: water; acetic acid / 8 h / 20 °C

3: pyridine / 10 h / 60 °C

With pyridine; tetrabutylammomium bromide; water; acetic acid; sodium hydroxide; In dichloromethane; water;
DOI:10.1002/adsc.201100988

Reference yield:

: 76-83-5
trityl chloride

: 392712-09-3
(1R)-1-[(3aR,5R,6S,6aR)-2,2-dimethyl-6-(prop-2-yn-1-yloxy)tetrahydro-2H-furo[2,3-d][1,3]dioxol-5-yl]ethane-1,2-diol

: 1402436-27-4
1-(2,2-dimethyl-6-prop-2-ynyloxytetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-trityloxyethanol

Guidance literature:: With pyridine; at 60 ℃; for 10h;
DOI:10.1002/adsc.201100988

Reference yield:

: 67441-18-3
(3aR,4S,5R,6aR)-5-(2,2-dimethyl-[1,3]dioxolan-4R-yl)-2,2-dimethyl-6-prop-2-ynyloxy-tetrahydrofuro[2,3-d][1,3]dioxole

: 1402436-27-4
1-(2,2-dimethyl-6-prop-2-ynyloxytetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-trityloxyethanol

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetic acid / 8 h / 20 °C

2: pyridine / 10 h / 60 °C

With pyridine; water; acetic acid;
DOI:10.1002/adsc.201100988