2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Base Information

Chemical Name:2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
CAS No.:1420376-59-5
Molecular Formula:C₁₇H₃₁O₅P
Molecular Weight:346.404
Hs Code.:

Synonyms:2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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Chemical Property of 2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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Technology Process of 2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

There total 3 articles about 2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(diethyl-phosphinoyl)-2-phenylselanyl-propionic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 1420376-59-5
2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: With dihydrogen peroxide; In dichloromethane; water; at 20 ℃; for 1.08333h; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.tetasy.2012.11.021

Reference yield:

: 141540-20-7
(diethoxy-phosphoryl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 1420376-59-5
2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / dimethyl sulfoxide / 0 - 20 °C / Inert atmosphere

1.2: 4 h / 60 °C / Inert atmosphere

2.1: dihydrogen peroxide / water; dichloromethane / 1.08 h / 20 °C / Inert atmosphere; Cooling with ice

With potassium tert-butylate; dihydrogen peroxide; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/j.tetasy.2012.11.021

Reference yield:

: 2216-51-5
(-)-menthol

: 1420376-59-5
2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / toluene / 48 h / 115 °C / Inert atmosphere

2.1: potassium tert-butylate / dimethyl sulfoxide / 0 - 20 °C / Inert atmosphere

2.2: 4 h / 60 °C / Inert atmosphere

3.1: dihydrogen peroxide / water; dichloromethane / 1.08 h / 20 °C / Inert atmosphere; Cooling with ice

With dmap; potassium tert-butylate; dihydrogen peroxide; In dichloromethane; water; dimethyl sulfoxide; toluene;
DOI:10.1016/j.tetasy.2012.11.021