[(1S,2R)-2-[(benzoyloxy)methyl]-1-(hydroxymethyl)cyclopropyl]methyl benzoate

Base Information

Chemical Name:[(1S,2R)-2-[(benzoyloxy)methyl]-1-(hydroxymethyl)cyclopropyl]methyl benzoate
CAS No.:145032-59-3
Molecular Formula:C₂₀H₂₀O₅
Molecular Weight:340.376
Hs Code.:

Synonyms:[(1S,2R)-2-[(benzoyloxy)methyl]-1-(hydroxymethyl)cyclopropyl]methyl benzoate

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Chemical Property of [(1S,2R)-2-[(benzoyloxy)methyl]-1-(hydroxymethyl)cyclopropyl]methyl benzoate

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Technology Process of [(1S,2R)-2-[(benzoyloxy)methyl]-1-(hydroxymethyl)cyclopropyl]methyl benzoate

There total 14 articles about [(1S,2R)-2-[(benzoyloxy)methyl]-1-(hydroxymethyl)cyclopropyl]methyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 144985-86-4
(1S,2R)-{2-[(benzoyloxy)methyl]-1-[(benzyloxy)methyl]cycloprop-1-yl}methyl benzoate

: 145032-59-3
[(1S,2R)-2-[(benzoyloxy)methyl]-1-(hydroxymethyl)cyclopropyl]methyl benzoate

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; for 72h; under 760 Torr; Ambient temperature;
DOI:10.1021/jm9705869

Reference yield: 60.0%

: 98-88-4
benzoyl chloride

: 389626-36-2
{(1R,2R)-2-(hydroxymethyl)-2-[(trityloxy)methyl]cyclopropyl}methanol

: 145032-59-3
[(1S,2R)-2-[(benzoyloxy)methyl]-1-(hydroxymethyl)cyclopropyl]methyl benzoate

Guidance literature:: benzoyl chloride; {(1R,2R)-2-(hydroxymethyl)-2-[(trityloxy)methyl]cyclopropyl}methanol; In pyridine; at 0 ℃; for 1h;

With formic acid; In diethyl ether; at 0 ℃; for 0.5h;
DOI:10.1016/S0040-4020(02)01002-5

Reference yield:

: 98-88-4
benzoyl chloride

: 145032-59-3
[(1S,2R)-2-[(benzoyloxy)methyl]-1-(hydroxymethyl)cyclopropyl]methyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / pyridine / CHCl₃

2: 99 percent / AcOH, H₂ / 10percent Pd/C / ethanol / 72 h / 760 Torr / Ambient temperature

With pyridine; hydrogen; acetic acid; palladium on activated charcoal; In ethanol; chloroform;
DOI:10.1021/jm9705869