sulfurous acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester

Base Information

Chemical Name:sulfurous acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester
CAS No.:911829-49-7
Molecular Formula:C₂₃H₃₄O₇S₂Si
Molecular Weight:514.736
Hs Code.:

sulfurous acid 3-(<i>tert</i>-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester

Synonyms:sulfurous acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester

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Chemical Property of sulfurous acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester

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Technology Process of sulfurous acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester

There total 1 articles about sulfurous acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 6378-11-6
ethyl chlorosulfite

: 125111-27-5
3-((tert-butyldiphenylsilyl)oxy)propane-1,2-diol

: 911829-49-7
sulfurous acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester

Guidance literature:: With pyridine; In ethyl acetate; at 0 ℃;
DOI:10.1021/jo060404v

Reference yield: 91.0%

: 911829-49-7
sulfurous acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester

: sulfuric acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfonyloxy-propyl ester ethyl ester

Guidance literature:: With sodium periodate; ruthenium trichloride; In methanol; dichloromethane; water; for 1h;
DOI:10.1021/jo060404v

Reference yield:

: 911829-49-7
sulfurous acid 3-(tert-butyl-diphenyl-silanyloxy)-2-ethoxysulfinyloxy-propyl ester ethyl ester

: 3-(tert-butyldiphenylsilyl)glycerol-1,2-disulfate disodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaIO₄ / RuCl₃ / CH₂Cl₂; methanol; H₂O / 1 h

2: 100 percent / NaI / acetone / 20 °C

With sodium periodate; sodium iodide; ruthenium trichloride; In methanol; dichloromethane; water; acetone;
DOI:10.1021/jo060404v