C₄₇H₅₂N₄O₉

Base Information

• Chemical Name: C₄₇H₅₂N₄O₉
• CAS No.: 947747-23-1
• Molecular Formula: C₄₇H₅₂N₄O₉
• Molecular Weight: 816.951
• Mol file: 947747-23-1.mol

Synonyms:C₄₇H₅₂N₄O₉

Chemical Property of C₄₇H₅₂N₄O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₇H₅₂N₄O₉

There total 13 articles about C₄₇H₅₂N₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C45H47N3O9 (947747-44-6) + N,0-dimethylhydroxylamine (1117-97-1) → C47H52N4O9 (947747-23-1)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

DOI:10.1016/j.tetlet.2007.05.161

Reference yield:

C42H40O5 (947747-20-8) → C47H52N4O9 (947747-23-1)

Guidance literature:

Multi-step reaction with 8 steps

1: 88 percent / pyridine

2: 94 percent / NaN₃ / dimethylformamide

3: 86 percent / PPTs / methanol

4: 64 percent / MeOTf / CH₂Cl₂

5: 81 percent / DDQ / CH₂Cl₂; methanol

6: 91 percent / TPAP; NMO; MS₄A / acetonitrile

7: 85 percent / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O

8: 90 percent / EDC*HCl / CH₂Cl₂

With sodium chlorite; sodium dihydrogenphosphate; sodium azide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; pyridinium p-toluenesulfonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl trifluoromethanesulfonate; In pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.tetlet.2007.05.161

Reference yield:

C42H39N3O4 (947747-21-9) → C47H52N4O9 (947747-23-1)

Guidance literature:

Multi-step reaction with 6 steps

1: 86 percent / PPTs / methanol

2: 64 percent / MeOTf / CH₂Cl₂

3: 81 percent / DDQ / CH₂Cl₂; methanol

4: 91 percent / TPAP; NMO; MS₄A / acetonitrile

5: 85 percent / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O

6: 90 percent / EDC*HCl / CH₂Cl₂

With sodium chlorite; sodium dihydrogenphosphate; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; pyridinium p-toluenesulfonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl trifluoromethanesulfonate; In methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.tetlet.2007.05.161

upstream raw materials:

C₄₅H₄₇N₃O₉

N,0-dimethylhydroxylamine

C₄₂H₄₀O₅

C₄₃H₄₂O₇S

Downstream raw materials:

C₅₉H₇₁N₃O₈

C₅₀H₅₃N₃O₈

(2S,3S,4R)-2-azido-3-benzyloxy-1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyloxy)octadec-5-yn-4-ol

C₅₀H₅₅N₃O₈