C₄₇H₅₈O₃Si

Base Information

Chemical Name:C₄₇H₅₈O₃Si
CAS No.:1452373-05-5
Molecular Formula:C₄₇H₅₈O₃Si
Molecular Weight:699.061
Hs Code.:

C<sub>47</sub>H<sub>58</sub>O<sub>3</sub>Si

Synonyms:C₄₇H₅₈O₃Si

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Chemical Property of C₄₇H₅₈O₃Si

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Technology Process of C₄₇H₅₈O₃Si

There total 6 articles about C₄₇H₅₈O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1452373-02-2
(S,E)-2-(2-(triisopropylsilyloxy)ethyl)-6-(trityloxy)hex-4-en-1-ol

: 939-26-4
2-bromomethylnaphthyl bromide

: 1452373-05-5
C₄₇H₅₈O₃Si

Guidance literature:: With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 12h; Inert atmosphere;
DOI:10.3762/bjoc.9.132

Reference yield:

: 142096-78-4
(E)-1-hydroxy-4-(triphenylmethoxy)-2-butene

: 1452373-05-5
C₄₇H₅₈O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

2.1: sodium iodide / acetone / 18 h / Darkness; Reflux; Inert atmosphere

3.1: n-butyllithium; lithium chloride; diisopropylamine / tetrahydrofuran; hexane / 1.33 h / -78 - 20 °C / Inert atmosphere

3.2: 2.5 h / 0 °C / Inert atmosphere

4.1: n-butyllithium; diisopropylamine; borane-ammonia complex / tetrahydrofuran; hexane / 0.83 h / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 12 h / 0 °C / Inert atmosphere

With n-butyllithium; borane-ammonia complex; sodium hydride; triethylamine; diisopropylamine; sodium iodide; lithium chloride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; acetone; mineral oil; 3.1: |Meyer Alkylation / 3.2: |Meyer Alkylation;
DOI:10.3762/bjoc.9.132

Reference yield:

: 1374423-85-4
C₂₄H₂₄O₄S

: 1452373-05-5
C₄₇H₅₈O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium iodide / acetone / 18 h / Darkness; Reflux; Inert atmosphere

2.1: n-butyllithium; lithium chloride; diisopropylamine / tetrahydrofuran; hexane / 1.33 h / -78 - 20 °C / Inert atmosphere

2.2: 2.5 h / 0 °C / Inert atmosphere

3.1: n-butyllithium; diisopropylamine; borane-ammonia complex / tetrahydrofuran; hexane / 0.83 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 12 h / 0 °C / Inert atmosphere

With n-butyllithium; borane-ammonia complex; sodium hydride; diisopropylamine; sodium iodide; lithium chloride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; acetone; mineral oil; 2.1: |Meyer Alkylation / 2.2: |Meyer Alkylation;
DOI:10.3762/bjoc.9.132