3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl

Base Information

Chemical Name:3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl
CAS No.:1201800-16-9
Molecular Formula:C₃₆H₅₄B₄O₈
Molecular Weight:658.064
Hs Code.:

Synonyms:3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl

Suppliers and Price of 3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl

Chemical Property:

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Technology Process of 3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl

There total 2 articles about 3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 92-52-4,1594-86-1
biphenyl

: 73183-34-3
bis(pinacol)diborane

: 1201800-16-9
3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl

Guidance literature:: bis(pinacol)diborane; With 4,4'-dimethyl-2,2'-bipyridines; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; potassium tert-butylate; In tetrahydrofuran; at 50 ℃; for 0.166667h; Inert atmosphere;

biphenyl; In tetrahydrofuran; at 85 ℃; for 96h; Inert atmosphere;
DOI:10.1021/ja307547j

Reference yield:

: 1201800-16-9
3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl

Guidance literature:

Reference yield: 64.0%

: 10495-73-5
2-bromo-6-(pyridin-2-yl)pyridine

: 1201800-16-9
3,5,3',5'-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl

: 1185738-83-3
3,5,3',5'-tetrakis(2,2'-bipyridin-6-yl)biphenyl

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 22h; Inert atmosphere; Reflux;