(E)-1-(3-hydroxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine

Base Information

Chemical Name:(E)-1-(3-hydroxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine
CAS No.:155106-27-7
Molecular Formula:C₁₇H₂₃NO₃
Molecular Weight:289.375
Hs Code.:

Synonyms:(E)-1-(3-hydroxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine

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Chemical Property of (E)-1-(3-hydroxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine

Chemical Property:

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Technology Process of (E)-1-(3-hydroxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine

There total 5 articles about (E)-1-(3-hydroxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 155106-26-6
(E)-1-(3-acetoxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine

: 155106-27-7
(E)-1-(3-hydroxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine

Guidance literature:: With potassium carbonate; In methanol; for 0.583333h;

Reference yield:

: 62012-15-1
1-(3-hydroxypropyl)pyrrolidin-2-one

: 155106-27-7
(E)-1-(3-hydroxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / pyridine / 5 h / 0 - 25 °C

2: 77 percent / phosphorus pentasulfide, sodium carbonate / tetrahydrofuran / 5 h

3: 2.) triphenylphosphine, triethylamine / 1.)a) 4 deg C, 21 h, b) CH₃CN, 2 h, 2.) CH₃CN, 2 h

With pyridine; diphosphorus pentasulfide; sodium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran;

Reference yield:

: 62012-14-0
1-(3-acetoxypropyl)pyrrolidin-2-one

: 155106-27-7
(E)-1-(3-hydroxypropyl)-2-(2-methoxy-6-methylbenzoyl)methylenepyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / phosphorus pentasulfide, sodium carbonate / tetrahydrofuran / 5 h

2: 2.) triphenylphosphine, triethylamine / 1.)a) 4 deg C, 21 h, b) CH₃CN, 2 h, 2.) CH₃CN, 2 h

With diphosphorus pentasulfide; sodium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran;