ethyl 3,4-di-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside

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Chemical Name:ethyl 3,4-di-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside
CAS No.:151508-21-3
Molecular Formula:C₄₉H₄₉NO₇
Molecular Weight:763.931
Hs Code.:

Synonyms:ethyl 3,4-di-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside

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Chemical Property of ethyl 3,4-di-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside

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Technology Process of ethyl 3,4-di-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside

There total 3 articles about ethyl 3,4-di-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 100-39-0
benzyl bromide

: 151508-17-7
ethyl 2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside

: 151508-21-3
ethyl 3,4-di-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; for 168h; Ambient temperature;
DOI:10.1016/S0040-4020(01)87962-X

Reference yield:

: 59465-62-2
ethyl 2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

: 151508-21-3
ethyl 3,4-di-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / pyridine / 18 h / 80 °C

2: 85 percent / 50percent aq. NaOH, Bu₄NHSO₄ / CH₂Cl₂ / 168 h / Ambient temperature

With pyridine; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane;
DOI:10.1016/S0040-4020(01)87962-X

Reference yield:

: 76-83-5
trityl chloride

: 151508-21-3
ethyl 3,4-di-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-6-O-trityl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / pyridine / 18 h / 80 °C

2: 85 percent / 50percent aq. NaOH, Bu₄NHSO₄ / CH₂Cl₂ / 168 h / Ambient temperature

With pyridine; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane;
DOI:10.1016/S0040-4020(01)87962-X