4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine

Base Information

Chemical Name:4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine
CAS No.:1163720-66-8
Molecular Formula:C₁₆H₁₉FN₄O₃
Molecular Weight:334.35
Hs Code.:

Synonyms:4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine

Suppliers and Price of 4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine

There total 5 articles about 4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1163720-60-2
4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-3-nitro-2-aminopyridine

: 1163720-66-8
4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In methanol; at 20 - 25 ℃; Large scale;

Reference yield:

: 911297-02-4
N-(2-fluoro-4-hydroxyphenyl)carbamic acid tert-butyl ester

: 1163720-66-8
4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.25 h / 20 °C / Inert atmosphere

1.2: 1 h / 110 °C

2.1: hydrogen / 10% palladium on activated charcoal / ethyl acetate; ethanol / 5 h

With hydrogen; sodium hydride; 10% palladium on activated charcoal; In ethanol; dimethyl sulfoxide; ethyl acetate; mineral oil;

Reference yield:

: 399-95-1
4-amino-3-fluorophenol

: 1163720-66-8
4-(4-N-(tert-butoxycarbonyl)amino-3-fluorophenoxy)-2,3-diaminopyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: indium(III) chloride / 2 h / 35 °C / Neat (no solvent)

2.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.25 h / 20 °C / Inert atmosphere

2.2: 1 h / 110 °C

3.1: hydrogen / 10% palladium on activated charcoal / ethyl acetate; ethanol / 5 h

With hydrogen; sodium hydride; indium(III) chloride; 10% palladium on activated charcoal; In ethanol; dimethyl sulfoxide; ethyl acetate; mineral oil;