5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-chlorophenyl 2-cyanoethyl phosphate)

Base Information

Chemical Name:5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-chlorophenyl 2-cyanoethyl phosphate)
CAS No.:82892-65-7
Molecular Formula:C₄₆H₄₂ClN₄O₁₀P
Molecular Weight:877.287
Hs Code.:

Synonyms:5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-chlorophenyl 2-cyanoethyl phosphate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-chlorophenyl 2-cyanoethyl phosphate)

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Technology Process of 5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-chlorophenyl 2-cyanoethyl phosphate)

There total 1 articles about 5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-chlorophenyl 2-cyanoethyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82902-24-7
5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine

: 109-78-4
3-Hydroxypropionitrile

: 15074-54-1
2-chlorophenyl dichlorophosphate

: 82892-65-7
5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-chlorophenyl 2-cyanoethyl phosphate)

Guidance literature:: With 1,2,3-triazole; triethylamine; Yield given. Multistep reaction; 1.) THF;
DOI:10.1021/ja00385a026

Reference yield: 85.0%

: 82892-65-7
5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-chlorophenyl 2-cyanoethyl phosphate)

: 82892-67-9
4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-cyanoethyl 2-chlorophenyl phosphate)

Guidance literature:: With benzenesulfonic acid;
DOI:10.1021/ja00385a026

Reference yield:

: 82892-65-7
5'-O-(methoxytrityl)-4-N-(benzyloxycarbonyl)-2'-deoxycytidine 3'-O-(2-chlorophenyl 2-cyanoethyl phosphate)

: 82892-75-9
C₆₂H₅₈Cl₂N₆O₁₇P₂

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 2percent benzenesulfonic acid

2: 80 percent / TPS-NT

With 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole; benzenesulfonic acid;
DOI:10.1021/ja00385a026