3-(2-iodosophenyl)-1,2-benzisoxazole hydroxybisulfate

Base Information

Chemical Name:3-(2-iodosophenyl)-1,2-benzisoxazole hydroxybisulfate
CAS No.:99763-28-7
Molecular Formula:C₁₃H₁₀INO₆S
Molecular Weight:435.196
Hs Code.:

Synonyms:3-(2-iodosophenyl)-1,2-benzisoxazole hydroxybisulfate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-iodosophenyl)-1,2-benzisoxazole hydroxybisulfate

Chemical Property:

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Technology Process of 3-(2-iodosophenyl)-1,2-benzisoxazole hydroxybisulfate

There total 3 articles about 3-(2-iodosophenyl)-1,2-benzisoxazole hydroxybisulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 99763-21-0
3-(2-iodophenyl)-1,2-benzisoxazole

: 99763-28-7
3-(2-iodosophenyl)-1,2-benzisoxazole hydroxybisulfate

Guidance literature:: With dihydrogen peroxide; In sulfuric acid; acetic anhydride; 1.) -15 deg C, 1 d, 2.) 20 deg C, 1 d.;
DOI:10.1007/BF00504396

Reference yield:

: 25187-00-2
2-iodobenzophenone

: 99763-28-7
3-(2-iodosophenyl)-1,2-benzisoxazole hydroxybisulfate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / NH₂OH*HCl, conc. H₂SO₄ / 3-methyl-butan-1-ol / 23 h

2: 70 percent / K₂S₂O₈ / H₂SO₄ / 3 h / -15 °C

3: 85 percent / 29percent H₂O₂ / H₂SO₄; acetic anhydride / 1.) -15 deg C, 1 d, 2.) 20 deg C, 1 d.

With dipotassium peroxodisulfate; sulfuric acid; hydroxylamine hydrochloride; dihydrogen peroxide; In i-Amyl alcohol; sulfuric acid; acetic anhydride;
DOI:10.1007/BF00504396

Reference yield:

: 99763-20-9
2-iodobenzophenone syn-oxime

: 99763-28-7
3-(2-iodosophenyl)-1,2-benzisoxazole hydroxybisulfate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / K₂S₂O₈ / H₂SO₄ / 3 h / -15 °C

2: 85 percent / 29percent H₂O₂ / H₂SO₄; acetic anhydride / 1.) -15 deg C, 1 d, 2.) 20 deg C, 1 d.

With dipotassium peroxodisulfate; dihydrogen peroxide; In sulfuric acid; acetic anhydride;
DOI:10.1007/BF00504396