p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne

Base Information

Chemical Name:p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne
CAS No.:117570-20-4
Molecular Formula:C₂₃H₂₅NO₅S
Molecular Weight:427.521
Hs Code.:

Synonyms:p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne

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Chemical Property of p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne

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Technology Process of p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne

There total 4 articles about p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 108275-35-0,117569-96-7,117570-18-0
hydroxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

: 98-59-9
p-toluenesulfonyl chloride

: 117570-20-4
p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne

Guidance literature:: 1.) pyridine, reflux, 48 h; 2.) reflux, 4 h, 2,4,6-collidine;
DOI:10.1016/S0040-4020(01)85897-X

Reference yield:

: oxo-4 methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

: 117570-20-4
p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol

2: 94 percent / 1.) pyridine, reflux, 48 h; 2.) reflux, 4 h, 2,4,6-collidine

With sodium tetrahydroborate; In methanol;
DOI:10.1016/S0040-4020(01)85897-X

Reference yield:

: 117569-99-0
(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 N,N-dimethylacetamide

: 117570-20-4
p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) trichloroacetonitrile, KHCO₃, 30 percent H₂O₂ / CH₂Cl₂ / Heating; 1.) r.t., 10 h; 2.) reflux, 10 h

2: 94 percent / 1.) pyridine, reflux, 48 h; 2.) reflux, 4 h, 2,4,6-collidine

With dihydrogen peroxide; potassium hydrogencarbonate; trichloroacetonitrile; In dichloromethane;
DOI:10.1016/S0040-4020(01)85897-X