epoxy-3,4α p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahyrodibenzofuranne

Base Information

• Chemical Name: epoxy-3,4α p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahyrodibenzofuranne
• CAS No.: 117570-22-6
• Molecular Formula: C₂₃H₂₅NO₆S
• Molecular Weight: 443.521

Synonyms:epoxy-3,4α p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahyrodibenzofuranne

Chemical Property of epoxy-3,4α p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahyrodibenzofuranne

Chemical Property:

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Technology Process of epoxy-3,4α p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahyrodibenzofuranne

There total 5 articles about epoxy-3,4α p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahyrodibenzofuranne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne (117570-20-4) → epoxy-3,4α p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahyrodibenzofuranne (117570-22-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 20h; Ambient temperature;

DOI:10.1016/S0040-4020(01)85897-X

Reference yield:

hydroxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne (108275-35-0,117569-96-7,117570-18-0) → epoxy-3,4α p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahyrodibenzofuranne (117570-22-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / 1.) pyridine, reflux, 48 h; 2.) reflux, 4 h, 2,4,6-collidine

2: 95 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 20 h / Ambient temperature

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1016/S0040-4020(01)85897-X

Reference yield:

oxo-4 methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne → epoxy-3,4α p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahyrodibenzofuranne (117570-22-6)

Guidance literature:

Multi-step reaction with 3 steps

1: NaBH₄ / methanol

2: 94 percent / 1.) pyridine, reflux, 48 h; 2.) reflux, 4 h, 2,4,6-collidine

3: 95 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 20 h / Ambient temperature

With sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;

DOI:10.1016/S0040-4020(01)85897-X

upstream raw materials:

p.toluenesulfonyloxy-6 N,N-dimethylcarboxamidomethyl-9bβ tetrahyro-1,2,4a,9b dibenzofuranne

hydroxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 N,N-dimethylacetamide

<(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide

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