4-PROPOXYCARBONYLPHENYLBORONIC ACID

Base Information

• Chemical Name: 4-PROPOXYCARBONYLPHENYLBORONIC ACID
• CAS No.: 91062-38-3
• Molecular Formula: C10H13BO4
• Molecular Weight: 208.02
• Hs Code.: 2931900090
• Mol file: 91062-38-3.mol

Synonyms:PROPYL 4-BORONOBENZOATE;(4-PROPOXYCARBONYL)BENZENEBORONIC ACID;4-PROPOXYCARBONYLPHENYLBORONIC ACID;AKOS BRN-0775;4-(Propoxycarbonyl)benzeneboronic acid 97%;(4-n-Propoxycarbonyl)benzeneboronic acid, 97%;4-Boronobenzoate

Chemical Property of 4-PROPOXYCARBONYLPHENYLBORONIC ACID

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 108-112°C
• Refractive Index: 1.522
• Boiling Point: 366.42 °C at 760 mmHg
• PKA: 8.01±0.16(Predicted)
• Flash Point: 175.405 °C
• PSA: 66.76000
• Density: 1.18g/cm³
• LogP: -0.06680
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

(4-Propoxycarbonyl)phenylboronicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi,Xn
• Statements: 22-36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (4-Propoxycarbonyl)phenylboronic acid

Technology Process of 4-PROPOXYCARBONYLPHENYLBORONIC ACID

There total 2 articles about 4-PROPOXYCARBONYLPHENYLBORONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

propan-1-ol (71-23-8) + 4-carboxyphenylboronic acid (14047-29-1) → (4-carbopropyloxy phenyl)dihydroxy borane (91062-38-3)

Guidance literature:

With hydrogenchloride;

DOI:10.1016/S0040-4020(01)99333-0

Reference yield:

→ (4-carbopropyloxy phenyl)dihydroxy borane (91062-38-3)

Guidance literature:

p-Carboxy-phenylborsaeure, Propanol <90grad, 1h, in Ggw. v. HCl>;

Reference yield:

(±)-2-(4-iodophenyl)-1,4-dioxaspiro[4.5]deca-6,9-dien-8-one (1443293-87-5) + (4-carbopropyloxy phenyl)dihydroxy borane (91062-38-3) → (±)-2-{4-(4-propoxycarbonyl)phenyl}-1,4-dioxaspiro[4.5]deca-6,9-dien-8-one

Guidance literature:

With bis(triphenylphosphine)palladium(II) chloride; caesium carbonate; In water; N,N-dimethyl-formamide; at 80 ℃; for 18h;

DOI:10.1016/j.ejmech.2013.05.030

upstream raw materials:

propan-1-ol

4-carboxyphenylboronic acid

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