(Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene

Base Information

Chemical Name:(Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene
CAS No.:519060-06-1
Molecular Formula:C₁₈H₂₂N₂O₄
Molecular Weight:330.384
Hs Code.:

Synonyms:(Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene

Suppliers and Price of (Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene

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Technology Process of (Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene

There total 7 articles about (Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 519060-05-0
(Z)-1-[(4'-methoxy-2',3'-dinitro)-phenyl]-2-[(3'',4'',5''-trimethoxy)-phenyl]ethene

: 519060-06-1
(Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene

Guidance literature:: With acetic acid; zinc; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.bmc.2016.01.007

Reference yield:

: 519060-05-0
(Z)-1-[(4'-methoxy-2',3'-dinitro)-phenyl]-2-[(3'',4'',5''-trimethoxy)-phenyl]ethene

: acetone - water

: 519060-06-1
(Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene

Guidance literature:: With sodium thiosulfate; In water;

Reference yield:

: 22996-21-0
4-methoxy-2-nitro-benzaldehyde

: 519060-06-1
(Z)-2-(2`,3`-diamino-4`-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethene

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; nitric acid / 2 h / 0 °C / Inert atmosphere

2.1: sodium hydride / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.2: 5 h / Inert atmosphere

3.1: acetic acid; zinc / 3 h / 20 °C / Inert atmosphere

With sulfuric acid; nitric acid; sodium hydride; acetic acid; zinc; In dichloromethane; 2.2: |Wittig Olefination;
DOI:10.1016/j.bmc.2016.01.007