4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:852568-11-7
Molecular Formula:C₄₉H₄₄ClNO₁₃S
Molecular Weight:922.406
Hs Code.:

Synonyms:4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Chemical Property of 4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Technology Process of 4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 1 articles about 4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl bromide

: 141342-83-8
phenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-1-deoxy-β-D-glucopyranoside

: 852568-11-7
4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at -40 ℃;
DOI:10.1055/s-2005-863751

Reference yield: 85.0%

: 2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl fluoride

: 852568-11-7
4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 852568-12-8
C₆₃H₅₇ClFNO₁₉

Guidance literature:: With 4 A molecular sieve; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; at 0 ℃;
DOI:10.1055/s-2005-863751

Reference yield: 79.0%

: 852568-11-7
4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 916225-67-7
tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside

: C₁₄₅H₁₅₁ClN₂O₃₆

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at -20 - -10 ℃;
DOI:10.1002/anie.200601128