tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside

Base Information

• Chemical Name: tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside
• CAS No.: 916225-67-7
• Molecular Formula: C₁₀₂H₁₁₃NO₂₃
• Molecular Weight: 1721.01
• Mol file: 916225-67-7.mol

Synonyms:tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside

Chemical Property of tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside

There total 1 articles about tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside → tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside (916225-67-7)

Guidance literature:

With 2,6-dimethylpyridine; thiourea; In N,N-dimethyl-formamide; at 70 ℃; for 1h;

DOI:10.1002/anie.200601128

Reference yield: 79.0%

4-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside (852568-11-7) + tetradecyl 2-O-benzoyl-3-O-(4-O-(2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-4,6-O-benzylidene-β-D-galactopyranoside (916225-67-7) → C145H151ClN2O36

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at -20 - -10 ℃;

DOI:10.1002/anie.200601128